SIF has a BRUKER DSX-300 solid state NMR spectrometer.
This can be used for the samples which do not dissolve
in common solvents.
The spectrometer is extensively used for Magic Angle
spinning studies. It has multinuclear facilities and
covers all the nuclei resonating between 44 -121 MHz.
Also available high temperature facility for Magic Angle
Spinning work in the range of 300 -363 K. The spinning
speeds of 10 -12 KHz is achievable. For angle dependent
studies in spinning experiments, there also exists
facility to vary the spinning angle from 0 - 90 degrees.
Non-spinning (wideline) work can be carried out in the
frequency range of 4 - 300 MHz in the temperature range
of 100 - 373 K. Please note that high resolution proton NMR
experiment accessories are not available with us at the moment.
Details of the Instrument:
Make and model: BRUKER DSX 300, NMR Spectrometer
Magnetic filed: 7.04 Tesla
Platform : Linux & X-Winnmr
Proton freq.: 300.013 MHz
Carbon freq.: 75.47 MHz
Important: Please supply 400 mg. of sample
in fine powder form.
Write your name, sample code, nucleus
to be studied on the container.
Please supply reference compound
for nuclei other than 13C and 29Si.